One-pot synthesis and characterization of biopolymer – Iron Oxide nanocomposite

Authors

  • A. Jegan. Department of Chemistry, Sona College of Technology, Salem, India.
  • A. Ramasubbu Department of Chemistry, Government Arts College (Autonomous), Coimbatore, India.
  • S. Saravanan Department of Chemistry, Sona College of Technology, Salem, India.
  • S. Vasanthkumar Department of Chemistry and nanotechnology, Karunya University, Coimbatore, India.
Abstract:

The magnetite (Fe3O4) – agar nanocomposite was prepared by co-precipitation of Fe (III) and Fe (II) ions for the first time. The obtained samples were characterized by x-ray diffraction, Fourier-transform infrared spectroscopy, scanning electron microscopy and transmission electron microscopy. FT-IR results confirm the formation of Fe3O4 nanoparticles in agar matrix. The XRD results revealed the presence of magnetite nanoparticles. The SEM results confirm that the magnetite nanoparticles are dispersed in the agar matrix. TEM micrograph clearly illustrates that the magnetite nanoparticles sizes varies from 50 – 200 nm.

Upgrade to premium to download articles

Sign up to access the full text

Already have an account?login

similar resources

one-pot synthesis and characterization of biopolymer – iron oxide nanocomposite

the magnetite (fe3o4) – agar nanocomposite was prepared by co-precipitation of fe (iii) and fe (ii) ions for the first time. the obtained samples were characterized by x-ray diffraction, fourier-transform infrared spectroscopy, scanning electron microscopy and transmission electron microscopy. ft-ir results confirm the formation of fe3o4 nanoparticles in agar matrix. the xrd results revealed th...

full text

One-pot synthesis of Ag/Fe3O4 nanocomposite: Preparation, characterization and efficient catalyst

In this study, nanometer sized of Ag/Fe3O4 nanocomposite (AFN) have been synthesized by using a simple and based on chemical reduction method. The size and shape of (AFN) controlled by using of condensation (Fe2O3 (2.975 mmol), NaBH4 (21.25 mmol), AgNO3 (2.532 mmol) and polyvinylpyrrolidone (PVP) (8.925 mmol K30 Mr=10.000) in 40 ºC. The synthesized AFN was characterized by XRD, scanning electro...

full text

One-pot Synthesis and Characterization of Highly Functionalized Thiazoles

A facile and efficient one-pot three-step process for the synthesis of 5-acetyl-2-imino-4-methylthiazoles via the cyclocondensation of 3-thiocyanatoacetylacetone with various hydrazine or hydrazide derivatives in EtOH has been developed. 3-Thiocyanatoacetylacetone itself has been synthesized as the intermediate from substitution reaction of thiocyanate with 3-chloroacetylacetone. B...

full text

synthesis and characterization of some macrocyclic schiff bases

ماکروسیکلهای شیف باز از اهمیت زیادی در شیمی آلی و دارویی برخوردار می باشند. این ماکروسیکلها با دارابودن گروه های مناسب در مکانهای مناسب می توانند فلزاتی مثل مس، نیکل و ... را در حفره های خود به دام انداخته، کمپلکسهای پایدار تولید نمایند. در این پایان نامه ابتدا یک دی آلدئید آروماتیک از گلیسیرین تهیه می شود و در مرحله بعدی واکنش با دی آمینهای آروماتیک و یا آلیفاتیک در رقتهای بسیار زیاد منجر به ت...

15 صفحه اول

Synthesis and characterization of zinc oxide – agar nanocomposite

A novel zinc oxide - agar nanocomposite was successfully synthesized using zinc chloride as a precursor. The nanocomposite was prepared using a domestic microwave oven. The prepared nanocomposites have been characterized by Fourier transform infrared (FTIR) spectroscopy, X-ray diffraction (XRD) analysis, scanning electron microscopy (SEM) and UV- visible spectroscopy. The crystalline properties...

full text

My Resources

Save resource for easier access later

Save to my library Already added to my library

{@ msg_add @}


Journal title

volume 2  issue Issue 2

pages  105- 110

publication date 2011-12-01

By following a journal you will be notified via email when a new issue of this journal is published.

Hosted on Doprax cloud platform doprax.com

copyright © 2015-2023